摘要 I
ABSTRACT II
目次 III
圖目次 VI
表目次 VIII
附錄 IX
縮寫表 X
第一章 前言 1
第二章 文獻回顧 3
2.1. 碳點 3
2.1.1. 簡介 3
2.1.2. 製備方法 3
2.2. 光學特性 4
2.2.1. UV-Vis吸收 5
2.2.2. 光致發光與其機制 5
2.2.3. 螢光穩定性 8
2.3. 量子產率 8
2.4. 螢光探針 8
2.4.1. 螢光淬滅(turn off) 9
2.4.2. 螢光恢復(turn off-on) 10
2.4.3. 螢光增加(turn on) 10
2.5. CD應用於抗生素檢測 11
2.5.1. 檢測抗生素之CD螢光探針 11
2.5.2. 檢測抗生素之CD結合金屬離子的螢光探針 11
2.5.3. 檢測抗生素之CD複合物 12
2.6. 奈米晶體 12
2.6.1. 幾丁質奈米晶體 12
2.6.2. 纖維素奈米晶體 13
2.7. 即時檢測OTC的傳感器 13
第三章 實驗材料 15
3.1. 實驗藥品 15
3.2. 儀器設備 16
第四章 實驗架構 18
第五章 實驗方法 19
5.1. CD製備 19
5.2. CD之特性分析 19
5.2.1. CD的粒徑與形態分析 19
5.2.2. 界達電位 19
5.2.3. 螢光與UV-Vis光譜 20
5.2.4. FT-IR分析 20
5.2.5. 量子產率 20
5.3. 影響CD螢光穩定性的因子 21
5.3.1. pH值 21
5.3.2. 鹽離子濃度 21
5.3.3. 溫度 21
5.4. CD應用於抗生素檢測 21
5.4.1. 檢測OTC之CD螢光探針 21
5.4.2. CD對不同金屬離子的選擇性 22
5.4.3. 檢測OTC之CD結合金屬離子螢光探針 22
5.5. 纖維素奈米晶體之製備 22
5.6. 幾丁質奈米晶體之製備 22
5.7. 纖維素和幾丁質奈米晶體特性之分析 23
5.7.1. TEM分析 23
5.7.2. XRD分析 23
5.7.3. FTIR分析 23
5.7.4. 介達電位 23
5.8. 即時檢測OTC之CD傳感器試片 24
5.8.1. 即時檢測OTC之CD/TLC試片 24
5.8.2. 即時檢測OTC之CD結合金屬離子/TLC試片 24
第六章 結果與討論 25
6.1. NCD-EA和NCD-EDA之特性分析 25
6.1.1. NCD-EA和NCD-EDA之粒徑分布與形狀 25
6.1.2. NCD-EA和NCD-EDA之電位 25
6.1.3. NCD-EA和NCD-EDA之FTIR圖譜 25
6.1.4. NCD-EA和NCD-EDA之UV-VIS吸收光譜 26
6.1.5. NCD-EA和NCD-EDA之螢光光譜 26
6.1.6. NCD-EA和NCD-EDA之量子產率 26
6.2. PH對CD螢光穩定性的影響 26
6.3. CD應用於抗生素檢測 27
6.4. 纖維素和幾丁質奈米晶體特性之分析 28
6.4.1. 纖維素和幾丁質奈米晶體長度分布與形狀 28
6.4.2. 纖維素和幾丁質奈米晶體之XRD和FTIR分析 29
6.4.3. 纖維素和幾丁質奈米晶體之電位 29
6.5. 即時檢測OTC之CD傳感器試片 30
6.5.1. 即時檢測OTC之CD/TLC試片 30
6.5.2. 即時檢測OTC之CD結合金屬離子/TLC試片 31
第七章 結論 32
參考文獻 33
第八章 圖 42
第九章 表 60
附錄 65

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